The distilling flask has an elongated neck so that Wurtz.
On the table were vodka, a flask of rum, white bread, roast mutton, and salt.
On distilling such a mixture under constant pressure, a mixture of the two components (of variable composition) will come over until there remains in the distilling flask the mixture of minimum vapour pressure.
It generally happens that much of the mercury column is outside the flask and consequently at a lower temperature than the bulb, hence a correction of the observed temperature is necessary.
The flask is again brought to room-temperature, and re-weighed.
The earliest form of Leyden jar consisted of a glass vial or thin Florence flask, partly full of water, having a metallic nail inserted through the cork which touched the water.
In its simplest form this is a hollow flask-shaped horny piece, consisting of a dilated basal portion and a terminal spiniform portion with an orifice at the apex; but its structure is frequently complicated by accessory processes and outgrowths which aid copulation and serve to protect the delicate point from injury.
The oxidation, which is effected by chromic acid and sulphuric acid, is conducted in a flask provided with a funnel and escape tube, and the carbon dioxide formed is swept by a current of dry air, previously freed from carbon dioxide, through a drying tube to a set of potash bulbs and a tube containing soda-lime; if halogens are present, a small wash bottle containing potassium iodide, and a U tube containing glass wool moistened with silver nitrate on one side and strong sulphuric acid on the other, must be inserted between the flask and the drying tube.
The genus Hevea was formerly called Siphonia, and the tree named Pao de Xerringa by the Portuguese, from the use by the Omaqua Indians of squirts or syringes made from a piece of pipe inserted in a hollow flask-shaped ball of rubber.
The inflorescence is a very simple one, consisting of one or two male flowers each comprising a single stamen, and a female flower comprising a flask-shaped pistil.
A condenser so placed that the condensed vapours return to the distilling flask, a device permitting the continued boiling of a substance with little loss; W.
The retort may be replaced by a distilling flask, which is a round-bottomed flask (generally with a lengthened neck) provided with an inclined side tube.
The neck of the retort, or side tube of the flask, is connected to the condenser c by an ordinary or rubber cork, according to the nature of the substance distilled; ordinary corks soaked in paraffin wax are very effective when ordinary or rubber corks cannot be used.
Nitrogen, carbon dioxide, &c., which is led in at the distilling flask before the process is started, and a slow current maintained during the operation.
The less volatile vapours are condensed and return to the flask,, while the more volatile component passes over.
The success of the operation depends upon two factors: (I) that the heating be careful, slow and steady, and (2) that the column attached to the flask be efficient to sort out, as it were, the most volatile vapour.
On distilling such a mixture, a mixture of constant composition will distil first, leaving in the distilling flask one or other of the components according to the composition of the mixture.
In some Gymnolaemata, polypides which develop an ovary possess a flask-shaped "intertentacular organ," situated between two of the tentacles, and affording a direct passage into the introvert for the eggs or even the spermatozoa developed in the same zooecium.
For volatile liquids, a flask provided with a long neck which carries a graduation and is fitted with a well-ground stopper is recommended.
The flask was then brought to o° by immersion in melting ice, the pressure of the gas taken, and the stop-cock closed.
The flask is removed from the ice, allowed to attain the temperature of the room, and then weighed.
The flask is now partially exhausted, transferred to the cooling bath, and after standing the pressure of the residual gas is taken by a manometer.
The volume of the flask is determined by weighing empty and filled with water.
The method differed from Regnault's inasmuch as the flask was exhausted to an almost complete vacuum,a performance rendered possible by the high efficiency of the modern air-pump. The actual experiment necessitates the most elaborate precautions, for which reference must be made to Morley's original papers in the Smithsonian Contributions to Knowledge (1895), or to M.
In 1826 Dumas devised a method suitable for substances of high boiling-point; this consisted in its essential point in vaporizing the substance in a flask made of suitable material, sealing it when full of vapour, and weighing.
Before the commercial production of calcium carbide made it one of the most easily obtainable gases, the processes which were most largely adopted for its preparation in laboratories were: - first, the decomposition of ethylene bromide by dropping it slowly into a boiling solution of alcoholic potash, and purifying the evolved gas from the volatile bromethylene by washing it through a second flask containing a boiling solution of alcoholic potash, or by passing it over moderately heated soda lime; and, second, the more ordinarily adopted process of passing the products of incomplete combustion from a Bunsen burner, the flame of which had struck back, through an ammoniacal solution of cuprous chloride, when the red copper acetylide was produced.
- Large Gold Human Figure, with a gold coco-flask in each hand; gold diadem, nose and ear ornaments, and chains on neck and legs.
In filtering into a vacuum the flask receiving the filtrate should be connected to the exhaust through a second flask.
Soc., 1862, p. 267) recommends melting the metal in a flask filled with nitrogen and gradually displacing this gas by oxygen; the first formed grey film on the metal changes to a deep blue, and then the gas is rapidly absorbed, the film becoming white and afterwards yellow.
Three old-established inns, the Bull and Bush, the Spaniards, and Jack Straw's Castle (the name of which has no historical significance), claim many great names among former visitors; while the Upper Flask Inn, now a private house, was the meeting-place of the Kit-Cat Club.
The female organ is essentially a flask-shaped structure; the neck of the flask growing out as the trichogyne, and the belly composed of an axial carpogenic cell surrounded by investing cells, and with one cell (trichophoric) between it and the trichogyne.
The tetrachloride, WC1 41 is obtained by partial reduction of the higher chlorides with hydrogen; a mixture of the pentaand hexa-chloride is distilled in a stream of hydrogen or carbon dioxide, and the pentachloride which volatilizes returned to the flask several times.
They found that the germ of tetanus had been introduced into the fluid before the bottle was opened at Malkowal, and they thought it probable that this might have occurred owing either to insufficient sterilization or to the process of filling the bottle from a larger flask having been performed with defective precautions.
In summer the club met at the Upper Flask, Hampstead Heath.
This form of fruit is succeeded by others which have received different names, and lastly by the mature Nectria which forms minute red flask-shaped perithecia on parts of the rotted potatoes that have dried up. The intermediate forms are known as Monosporium, Fusarium and Cephalosporium.
In the electrolytic method from o 5 to 5 grammes of ore are treated in a flask or beaker, with a mixture of io cc. of nitric and ro cc. of sulphuric acid, until thoroughly decomposed.
One gramme of the ore is treated in a flask with a mixture of nitric and sulphuric acids and evaporated until all the nitric acid is expelled.
One gramme of ore is usually taken for assay and treated in a small flask or beaker with 10 cc. of hydrochloric acid.
In the reduction by metallic zinc, about 3 grammes of granulated or foliated zinc are placed in the flask, which is closed with a small funnel; when the iron is reduced, add 10 cc. of sulphuric acid, and as soon as all the zinc is dissolved the solution is ready for titration.
5 of a gramme of pure iron wire in a flask, in hydrochloric acid, oxidizing it with a little potassium chlorate, boiling off all traces of chlorine, deoxidizing by one of the methods described above, and titrating with the solution.
Soc., 1900, 77, p. 648) prepares pure hydrobromic acid by covering bromine, which is contained in a large flask, with a layer of water, and passing sulphur dioxide into the water above the surface of the bromine, until the whole is of a pale yellow colour; the resulting solution is then distilled in a slow current of air and finally purified by distillation over barium bromide.
Phosphorous acid, P(OH) 3, discovered by Davy in 1812, may be ' obtained by dissolving its anhydride, P 4 0 61 in cold water; by immersing sticks of phosphorus in a solution of copper sulphate contained in a well-closed flask, filtering from the copper sulphide and precipitating the sulphuric acid simultaneously formed by baryta water, and concentrating the solution in vacuo; or by passing chlorine into melted phosphorus covered with water, the first formed phosphorus trichloride being decomposed by the water into phosphorous and hydrochloric acids.
A simpler arrangement, also employed by Tyndall, is to cause the rays to be reflected outwards parallel to one another, and to concentrate them by means of a small flask, containing the iodine solution and used as a lens, placed some distance from the camera.
The neck of the flask-shaped pollen-chamber projected a little from the micropyle and no doubt received the pollen directly.
A Cossack who accompanied him had handed him a knapsack and a flask, and Nesvitski was treating some officers to pies and real doppelkummel.
Let's dwink to dwown our gwief! shouted Denisov, who had settled down by the roadside with a flask and some food.
This method did not give very certain results, for it could not be guaranteed that the growth in the inoculated flask was necessarily derived from a single bacterium.
(2) The preparation of the solution of the substance consists in dissolving an accurately determined weight, and making up the volume in a graduated cylinder or flask to a known volume.
Nitrobenzene, air cooling of the retort neck or of a straight tube connected with the distilling flask will suffice; or wet blotting-paper placed on the tube and the receiver immersed in water may be used.
Practically any vessel may serve as a receiver - test tube, flask, beaker, &c. If noxious vapours come over, it is necessary to have an air-tight connexion between the condenser and receiver, and to pro vide the latter with an outlet tube leading to an absorption column or other contrivance in which the vapours are taken up. If the substances operated upon decompose when heated in air, as, for example, the zinc alkyls which inflame, the air within the apparatus is replaced by some inert gas, e.g.
The titration is complete when the blue colour is so faint that it is almost imperceptible after the flask has been vigorously shaken.