A fine oil of turpentine is distilled from the crude material; the residue forms a coarse resin.
A spirit has been distilled from acorns in process of germination, when the saccharine principle is most abundant.
When distilled with phosphoric anhydride they yield nitriles.
It is also formed when ortho-aminodiphenylamine is distilled over lead peroxide (0.
The precipitated tellurium is then fused with potassium cyanide, the melt extracted with water and the element precipitated by drawing a current of air through the solution and finally distilled in a current of hydrogen.
Their abdominal bones are like those of the marsupials; and they are furnished with pouches for their young, but have no teats, the milk being distilled into their pouches from the mammary glands.
The juice, when not boiled down to form sugar, is either drunk fresh, or fermented and distilled to form arrack.
Distilled water is a very bad conductor, though, even when great care is taken to remove all dissolved bodies, there is evidence to show that some part of the trace of conductivity remaining is due to the water itself.
It is decomposed, on dry distillation, into carbon dioxide and pyromellitic acid, C i oH 6 0 8 i when distilled with lime it gives carbon dioxide and benzene.
As the carbon content of the molecule increases, they become less soluble in water, and their smell becomes less marked with the increase in boiling point, the highest members of the series being odourless solids, which can only be distilled without decomposition invacuo.
Paraldehyde is moderately soluble in water, and when distilled with sulphuric acid is reconverted into the ordinary form.
Hofmann is as follows: the mixture is distilled with caustic potash, when the primary, secondary and tertiary amines distil over, and the quaternary ammonium salt remains behind unaffected.
The plummet is now placed in distilled water at 15°, and the beam brought to equilibrium by means of a rider, which we shall call I, hung on a hook; other riders are provided,;nth and ii b th respectively of I.
When zoological records failed, Egypto-Hellenic ingenuity was never at a loss for a fanciful invention distilled from the text itself, but which to succeeding copyists appeared as part of the teaching of the original Physiologus.
Of mercury, and, when of specific gravity 1.295 (corresponding to about 80% of glycerin), it is distilled under a vacuum of 28 to 29 in.
Other leading manufactures are malt liquors ($21,620,794 in 1905), railway rolling-stock consisting largely of cars ($21,428,227), men's clothing ($18,496,173), planing mill products ($17,725,711), carriages and wagons ($16,096,125), distilled liquors ($15,976,523), rubber and elastic goods ($15,963,603), furniture ($13,322,608), cigars and cigarettes ($13,241,230), agricultural implements ($12,891,197), women's clothing ($12,803582), lumber and timber products ($12,567,992), soap and candles.
Ragozin states in his work on the petroleum industry that Johann Lerche, who visited the Caspian district in 1735, found that the crude Caucasian oil required to be distilled to render it satisfactorily combustible, and that, when distilled, it yielded a bright yellow oil resembling a spirit, which readily ignited.
In most petroleum-producing countries, however, and particularly where the product is abundant, the crude oil is fractionally distilled, so as to separate it into petroleum spirit of various grades, burning oils, gas oils, lubricating oils, and (if the crude oil yields that product) paraffin.
The charge was distilled almost to dryness, though the operation was not carried far enough to cause the residue to " coke."
In the earlier stages of the development of the manufacture of mineral lubricating oils, the residues were distilled in cast-iron stills, and the lubricating properties of the products thus obtained were injured by overheating.
In the routine examination of crude petroleum it is customary to determine the specific gravity, and the amount of water and earthy matter in suspension; the oil is also frequently subjected to a process of fractional distillation in order to ascertain whether there has been any addition of distilled products or residue.
The corresponding decomposition of a glyceride into an acid and glycerin takes place when the glyceride is distilled in superheated steam, or by boiling in water mixed with a suitable proportion of caustic potash or soda.
Beer and distilled liquors are largely manufactured, and fine building stone is obtained from numerous quarries.
The crude product is very impure and possesses an offensive smell; it may be purified by forcing a fine spray of lime water through the liquid until the escaping water is quite clear, the washed bisulphide being then mixed with a little colourless oil and distilled at a low temperature.
The residue is then fused with caustic potash and nitre, dissolved in water, saturated with chlorine and distilled on the water-bath in a current of chlorine.
The only manufacturing industries of much importance are the preparation of sugar, coffee and tobacco for market, and the manufacture of cigars, cigarettes, straw hats, soap, matches, vermicelli, sash, doors, ice, distilled liquors and some machinery.
Hofmann and Schotensack decompose a mixture of phenol (3 molecules) and sodium carbonate (4 mols.) with carbonyl chloride at 140-zoo° C. When 90% of the phenol has distilled over, the residue is dissolved and hydrochloric acid added, any phenol remaining is blown over in a current of steam, and the salicylic acid finally precipitated by hydrochloric acid.
In these marshes grows the nipa palm, from which a liquor is distilled - there are a number of small distilleries here.
Perfectly pure distilled sea-water dissociates, to an infinitesimal degree, into hydrogen (H) and hydroxyl (HO) ions, so that one litre of such water contains 1 X 10 7, or 1 part of a gram-molecule of either hydr010,000,000 gen or hydroxyl (a gramme-molecule of hydrogen is 2 grammes, or of hydroxyl 17 grammes).
Of the several individual chlorides, the following are liquids or solids, volatile enough to be distilled from glass vessels: AsC13, SbC1 3, SnCl 4, BiCl 3, HgC1 2, the chlorides of arsenic, antimony, tin, bismuth, mercury respectively.
Metallurgy The principles underlying the extraction of zinc may be summarized as: (I) the ore is first converted into zinc oxide; (2) the oxide is distilled with carbon and the distillate of metallic zinc condensed.
Moissan (ibid., 5906, 142, p. 673) has distilled this metal in a very intense electric furnace.
The tertiary amine is then distilled off, the residual products separated by filtration and finally hydrolysed by a caustic alkali.
The silver iodide is separated and the solvent distilled off.
The Arabians greatly improved the earlier apparatus, naming one form the alembic; they discovered many ethereal oils by distilling plants and plant juices, alcohol by the distillation of wine, and also distilled water.
The neck of the retort, or side tube of the flask, is connected to the condenser c by an ordinary or rubber cork, according to the nature of the substance distilled; ordinary corks soaked in paraffin wax are very effective when ordinary or rubber corks cannot be used.
This method is particularly successful in the case of substances which cannot be distilled at their ordinary boiling-points (it will be seen in the following section that distilling with steam implies a lowering of boiling-point), and which can be readily separated from water.
Instances of its application are found in the separation of orthoand para-nitrophenol, the o-compound distilling and the p- remaining behind; in the separation of aniline from the mixture obtained by reducing nitrobenzene; of the naphthols from the melts produced by fusing the naphthalene monosulphonic acids with potash; and of quinoline from the reaction between aniline, nitrobenzene, glycerin, and sulphuric acid (the product being first steam distilled to remove any aniline, nitrobenzene, or glycerin, then treated with alkali, and again steam distilled when quinoline comes over).
The above theory, coupled with such facts as the variation of the composition of the constant boiling-point fraction with the pressure under which the mixture is distilled, the proportionality of the density of all mixtures to their composition, &c., shows this to be erroneous.
Distillation in a vacuum is practised in two forms: - if the pump draws off steam as well as air it is termed a "wet" air-pump; if it only draws off air, it is a "dry" air-pump. In the glycerin industry the lyes obtained by saponifying the fats are first evaporated with "wet vacuum" and finally distilled with closed and live steam and a "dry vacuum."
The details of the plant - the material and fittings of the still, the manner of heating, the form of the condensing plant, receivers, &c. - have to be determined for each substance to be distilled in order to work with the maximum economy.
- Distilled water, i.e.
Rum is a by-product of the sugar industry, and "mescal" is distilled from the agave.
The calcium salts distilled with calcium formate yield aldehydes r distilled with soda-lime, ketones result.
Devoting himself to the economic side of geology in various parts of North America, he was enabled to bring out in 1861 A Practical Treatise on Coal, Petroleum and other Distilled Oils.
Eau de vie (" elixir of life") was in use during the 13th and 14th centuries; Arnoldus Villanovanus applied it to the product of distilled wine, though not as a specific name.
Their favourite drink is thong, distilled from rice or barley and millet, and Marwa, beer made from fermented millet.
O% over the value of the factory products in 1900; among its manufactures are tobacco, cigars, chewing tobacco and snuff (value in 1905, $2,879,217), patent medicines (value in 1905, $2,133,198), flour and grist mill products ($1,089,910), men's clothing ($ 8 33, 8 35), and, of less importance, commercial and computing scales and time recorders, chemicals, distilled liquor, beer, fire-alarm apparatus, overalls, agricultural implements, wagons, electrical apparatus, refined oil, sheet metal, paper bags and envelopes, tacks and nails, window glass, glass-ware, clocks, whips and furniture (especially Morris chairs).
The bottle is carefully cleansed by washing with soda, hydrochloric acid and distilled water, and then dried by heating in an air bath or by blowing in warm air.
A small stool is then placed over the balance pan, and on this is placed a beaker of distilled water so that the solid is totally immersed.
The acid, when distilled slowly, is decomposed and yields a and 0-angelica lactones.
The two last classes number over 400,000 (1903), but the quantity of alcohol distilled by them is small.
It is a white crystalline solid of melting point 43° C.; it boils at 210° C., and it can be distilled without decomposition.
When distilled over lead oxide, it forms diphenylene oxide, (C 6 H 4) 2 O: and when heated with oxalic acid and concentrated sulphuric acid, it forms aurin, C19H1403.
The simplest modes of preparing pure glycerin are based on the saponification of fats, either by alkalis or by superheated steam, and on the circumstance that, although glycerin cannot be distilled by itself under the ordinary pressure without decomposition, it can be readily volatilized in a current of superheated steam.
Pliny says that their wood was everlasting, and therefore images of the gods were made of it; he makes mention also of the oil of cedar, or cedrium, distilled from the wood, and used by the ancients for preserving their books from moths and damp; papyri anointed or rubbed with cedrium were on this account called ced ati libri.
In general, when the substance to be distilled has a vapour pressure of only 10 mm.
Journalist Brooks Atkinson, said: "After each war, there is a little less democracy left to save."