If the precipitate settles readily, the supernatant liquor may be decanted through the filter paper, more water added to the precipitate and again decanted.
The decanted ley deposits on standing a 70% potassium chloride, which is purified by washing with cold water.
Every twenty-four hours or so the flow of juice may be conveniently stopped, and, after all the impurities have subsided, the superincumbent clear liquor may be decanted by a cock placed at the side of the cone for the purpose, and the vessel may be washed out.
This powder is then lixiviated with hot water, the liquor decanted, and the alum allowed to crystallize.
Water is added, and as soon as the gangue and copper particles have settled the clear solution is decanted, and the residue washed several times in the same way.
The liquid is then allowed to stand for twelve hours, and the c.ear alcoholic solution is decanted from the precipitated hippuramide.
7764 (1890)] decomposes sulphocyanides by fusing with zinc: the zinc is heated with a small quantity of carbon and when completely fused potassium sulphocyanide is added, the mass being well stirred and heated until it thickens and begins to turn red; finally it is allowed to cool out of contact with air, lixiviated with water, the solution decanted, and evaporated to a paste in vacuo.
The simple siphon is used by filling it with the liquid to be decanted, closing the longer limb with the finger and plunging the shorter into the liquid; and it must be filled for each time of using.
It is now allowed to stand for some time, decanted from any sediment, and finally mixed with the calculated quantity of potassium sulphate (or if ammonium alum is required, with ammonium sulphate), well agitated, and the alum is thrown down as a finely-divided precipitate of alum meal.
It is insoluble in water and in nitric acid and apparently so in hydrochloric acid; but if heated with this last for some time it passes into a compound, which, after the acid mother liquor has been decanted off, dissolves in water.