She tried to think of a retort, but couldn't.
The retorts are charged with molten sulphur from an upper reservoir, which is kept at the requisite temperature by means of the lost heat of the retort fires.
The only excuse made for the alternate cringing and insult, the alternate abuse and lying, which marked his course in this matter, has been the very weak plea that a man cannot fight with a system - a plea which is sufficiently answered by the retort that a great many men have so fought and have won.
She opened her mouth to retort but stopped.
Sofia bit back a retort and forced herself to her feet.
"Yes, but she's…" Kiki's retort drifted off.
Each retort is provided with two adapters, namely, a conical pipe of fire-clay, about 15 in.
Be provided with a tubulure, or opening, which permits the charging of the retort, and also the insertion of a thermometer b.
The retort may be replaced by a distilling flask, which is a round-bottomed flask (generally with a lengthened neck) provided with an inclined side tube.
Jenn bit back a retort and left, unable to shake the sense he'd told her something he didn't mean for her to know.
The substance is heated in a retort a, which consists of a large bulb drawn out at the top to form a long neck; it may also FIG.
These have now to pass down the heated retort on their way to the ascension pipe, and the contact with the heated sides of the retort, and the baking from the radiant heat in the retort, set up an infinity of changes.
The retort is pear-shaped, and holds1000-1500lb of charge, consisting of liquated crust mixed with 1-3% of charcoal.
The neck of the retort, or side tube of the flask, is connected to the condenser c by an ordinary or rubber cork, according to the nature of the substance distilled; ordinary corks soaked in paraffin wax are very effective when ordinary or rubber corks cannot be used.
Sodium phenolate is heated in a stream of carbon dioxide in an iron retort at a temperature of 180-220° C., when half the phenol distils over and a basic sodium salicylate is left.
The effect produced by alteration in the temperature of the retort upon the composition of both gas and tar is very marked.
Prior to about the 18th century three forms of distillation were practised: (I) destillatio per ascensum, in which the retort was heated from the bottom, and the vapours escaped from the top; (2) destillatio per latus, in which the vapours escaped from the side; (3) destillatio per descensum, in which the retort was heated at the top, and the vapours led off by a pipe passing through the bottom.
The gas developed by the coal near the mouth of the retort is quickly washed out into the ascension pipe by the push of the gas behind, and the period for which it has been exposed to the radiant heat from the walls of the retort is practically nil; whilst the gas evolved in the portion of the retort farthest from the mouthpiece has only its own rate of evolution to drive it forward, and has to traverse the longest run possible in tile retort, exposed during the whole of that period to radiant heat and to contact with the highly heated surface of the retort itself.
Brady chewed back a retort about how this particular army-type had been battling insurgents to reach them on the Peak.
In such a case, the best retort was to return in all haste in order to put more energy into the huge centralized organism which the emperor alone could work.
Stannic Chloride, SnC1 4, named by Andreas Libavius in 1605 Spiritus argenti vivi sublimate from its preparation by distilling tin or its amalgam with corrosive sublimate, and afterwards termed Spiritus fumans Libavii, is obtained by passing dry chlorine over granulated tin contained in a retort; the tetrachloride distils over as a heavy liquid, from which the excess of chlorine is easily removed by shaking with a small quantity of tin filings and re-distilling.
Trans., 1869, p. 173) by decomposing the double fluoride of hydrogen and potassium, at a red heat in a platinum retort fitted with a platinum condenser surrounded by a freezing mixture, was having a platinum receiver luted on.
In practice the theoretical quantity of acid and Chile saltpetre is not used, but the charge is so regulated that the mixture of acid and neutral sodium sulphate formed in the retort remains liquid at the temperature employed, and consequently can be readily removed.
From this it will be seen that, with the increase of temperature, the hydrocarbons - the olefines and marsh gas series - gradually break up, depositing carbon in the crown of the retort, and liberating hydrogen, the percentage of which steadily increases with the rise of temperature.
Retort, the coal following banking up until an even layer is formed throughout the length of the retort.
Before it can be cupelled it has to be freed from most of the zinc, which is accomplished by distilling in a retort made of a mixture similar to that of the plumbago crucible.
Long, which fits into the retort end, and a conical tube of sheet iron, which fits over the end of the fire-clay pipe, and which at its outlet end is only about an inch wide.
The thermometer is placed so that the bulb is near the neck of the retort or the side tube of the distilling flask.
Nitrobenzene, air cooling of the retort neck or of a straight tube connected with the distilling flask will suffice; or wet blotting-paper placed on the tube and the receiver immersed in water may be used.
The most favourable retort is a shallow iron pan heated in a sand bath, and provided with a screwed-down lid bearing the delivery tube.
For the distillation of liquids the retort is usually a cylindrical pot placed vertically; cast iron is generally employed, in which case the bottom is frequently incurved and thicker than the sides in order to take up the additional wear and tear.
16) in which this wonderful process is carried out is a huge retort, lined with clay, dolomite or other refractory material, hung aloft and turned on trunnions, DD, through the right-hand one of which the blast is carried to the gooseneck E, which in turn delivers it to the tuyeres Q at the bottom.
The rest of the apparatus (settler, retort, crucible, furnace) is the same as with the Washoe process.
If the retorts are at a temperature of 1000° C. when the charge of coal is put in, the temperature of the distillation will vary from about 800° C. close to the walls, to about 400° C. in the centre of Effect of the coal; and in the same way, in the space above the coal, tempera- the products which come in contact with the sides of the tore in the retort are heated to 1000° C., whilst the gas near the coal retort.
Is probably heated to only 600° C. Moreover, the gases and vapours in the retort are subjected to a period of heating which varies widely with the distance from the mouth of the retort of the coal that is undergoing carbonization.
Of the first class, the light paraffin oils and pitch may be taken as examples; whilst benzene, naphthalene and retort carbon represent the second.
Wright found, in a series of experiments, that, when four portions of the same coal were distilled at temperatures ranging from a dull red heat to the highest temperature attainable in an iron retort, he obtained the following results as to yield and illuminating power: - Composition of the Gas.
They may be divided into - (a) Solids, such as the coke and retort carbon; (b) liquids, consisting of the tar and ammoniacal liquor; and (c) gases, consisting of the unpurified `coal gas.
The life of this retort is about thirty working months.
A cast iron mouthpiece and lid is bolted to the exterior end of each retort, the mouthpiece carrying a socket end to receive the ascension pipe, through which the gas passes on leaving the retort.
With this method it is necessary that the rake should enter and discharge several times before the retort is clear, and thus the use of a telescopic ram worked by hydraulic power, which pushes the coke before it and discharges it at the other end, is an advantage.
As each retort in a furnace is in all essentials a separate crucible, and as the metal from only a few of them goes into a single ingot, there can be no uniformity either in the ingots made from the same furnace during a day's run or in those made from several furnaces treating the same ore.
The apparatus consists of three parts: - the "retort" or "still," in which the substance is heated; the "condenser," in which the vapours are condensed; and the "receiver," in which the condensed vapours are collected.
This retort was President Kruger's rallying cry whenever he found himself in the least degree pressed, either from within or without the state.
The anodes are made of retort-carbon or other chlorine-resisting material, and they are mounted in cells which serve as diaphragms. The material of these cells is usually cement, mixed with certain soluble salts which impart sufficient porosity to the material.
When the rock has been separated from the amalgam by a washing operation, the quicksilver is recovered by distillation in an iron retort, and the remaining crude retortsilver melted into bars and shipped to a refinery, which removes the impurities, the leading one of which is copper.
Between the two middle toes, in most species, is lodged a deep glandular bag having the form of a retort with a small external orifice, which secretes an unctuous and odorous substance.
On submitting a complex substance of this character to destructive distillation, it will be found that the yield and quality of the products will vary very considerably with the temperature existing in the retorts, with the size of the charge of coal used, with its distribution in the retort, with the length of time the distillation has been going on, and with an infinity of other factors of a more or less complex nature.
The retort carbon products* formed as a dense deposit on the crown of the retort by the action of the high temperature on the hydrocarbons is, however, carbon in a very pure form, and, on account of its density, is largely used for electrical purposes.
When hydraulic pressure to the amount of 2000 to 3000 lb per square inch is applied, the saving is unquestioned, since less time is required to dry the pressed retort, its life in the furnaces is longer, its absorption of zinc is less, and the loss of zinc by passage through its walls in the form of vapour is reduced.
If a more dilute acid than this be distilled, water passes over in excess and the residue in the retort reaches the above composition and boiling point; on distillation of a stronger acid, excess of acid passes into the distillate and the boiling point rises until the values of the constant boiling mixture are reached.
Lange; as a retort to that writer's overbearing criticism, Lessing exposed with scathing satire Lange's errors in his popular translation of Horace.
Restored to the regency, Albany permitted his son, Murdoch, with Douglas, to retort on a successful raid by Percy and the traitor March.
There is very little doubt that the general course of the decompositions follows these iines; but any such simple explanation of the actions taking place is rendered impossible by the fact that, instead of the breaking-down of the hydrocarbons being completed in the coal, and only secondary reactions taking place in the retort, in practice the hydrocarbons to a great extent leave the coal as the vapours of condensible hydrocarbons, and the breaking down of these to such simple gaseous compounds as ethylene is proceeding in the retort at the same time as the breaking up of the ethylene already formed into acetylene and methane, and the polymerization of the former into higher compounds.
The retorts in which the coal is carbonized are almostluniversally made of fire-clay, and in all but small country works the old singleended retort, which was about 9 ft.
The iron adapters are now slipped on, and left on for two hours, when, as a matter of experience, a considerable amount of zinc has gone out of the retort, the greater part into the fire-clay adapter, the rest into the iron cone.
After solution the retort is gently heated by warm water when the gasisliberated: 3KC10 3 +2H 2 SO 4 = KC104+2KHS04+H20+C102.
The charging machines travel on lines in front of the retort bench, and the power is transmitted by connexions made with flexible hose.
As much as one-third on each ton of coal carbonized is saved by the use of machinery in the retort-house.
Below each retort, and attached to it, is a cooler formed of thin sheet-iron, which receives the hot char as it passes from the retort, and at the bottom of the cooler is an arrangement of valves which permits a certain amount of char to drop out and no more.
For the purpose of discharging the coke from the retort either compressed air or hydraulic machinery is employed, a rake being made to enter the retort and withdraw the coke on returning.
In the first two cases a scoop, filled with coal from an overhead hopper carried by the travelling machine, is made to enter the retort and is turned over; the operation is then repeated, but this time the scoop is turned over in the opposite direction, the coal thus assuming such a position that as much of its under surface as possible is exposed to the heated side of the retort.