These are washed with ammonium chloride until the filtrate is colourless, ignited, fused with caustic potash and nitre, the melt dissolved in water and nitric acid added to the solution until the colour of potassium ruthenate disappears.
I was dragged to my feet from behind by my captor as police burst through the door and the room ignited with the blinding glow of several flash lights.
A spark of the old humor ignited in the amber eyes and she canted her head toward her father.
A precipitate of ruthenium oxide gradually separates; this is collected and ignited in a graphite crucible and finally fused in the oxyhydrogen furnace (H.
The precipitate obtained is filtered, well washed with hot water, dried and then ignited until the weight is constant.
This uranate when ignited in a platinum crucible leaves a green oxide of the composition U308, i.e.
When ignited in a current of hydrogen it yields tiianium trifluoride, TiF 3, as a violet powder.
The residue so obtained is then powdered and ignited with barium nitrate, which converts the iridium into its oxide and the osmium into barium osmiate.
This is then dissolved in water, reduced by alcohol and ignited in oxygen.
(a) Gravimetric. - This method is made up of four operations: (I) a weighed quantity of the substance is dissolved in a suitable solvent; (2) a particular reagent is added which precipitates the substance it is desired to estimate; (3) the precipitate is filtered, washed and dried; (4) the filter paper containing the precipitate is weighed either as a tared filter, or incinerated and ignited either in air or in any other gas, and then weighed.
Zinc may be quantitatively estimated by precipitating as basic carbonate, which is dried and ignited to zinc oxide.
The pure salt is dissolved in hot water and decomposed with ammonia to produce a slightly ammoniacal hydrated oxide; this, when ignited in platinum, leaves pure TiO 2 in the form of brownish lumps, the specific gravity of which varies from 3.9 to 4.25, according to the temperature at which it was kept in igniting.
It is purified by boiling with acids, to remove any mineral matter, and is then ignited for a long time in a current of chlorine in order to remove the last traces of hydrogen.
The liquors are evaporated to dryness and the residue is ignited to obtain a very impure carbonate, which is purified by methods founded on the different solubilities of the several components.
A peculiarity of larch wood is the difficulty with which it is ignited, although so resinous; and, coated with a thin layer of plaster, beams and pillars of larch might probably be found to justify Caesar's epithet " igni impenetrabile lignum "; even the small branches are not easily kept alight, and a larch fire in the open needs considerable care.
The oil for ink-making is prepared by heating it in an iron pot up to the point where it either takes fire spontaneously or can be ignited with any flaming substance.
The residue in the filter is ignited and fused with a little sodium carbonate and nitrate, or with sodium peroxide.
Edith at first looked shocked, but almost at once, her face melted to a resigned look—a condemned maiden mounting the guillotine steps, Joan of Arc as the match ignited her pyre.
It fuses easily in the electric arc. It oxidizes superficially when heated, but fairly rapidly when ignited in an oxidizing blowpipe flame, forming a black smoke of the oxide.
The oxidizing agent in commonest use is copper oxide, which must be freshly ignited before use on account of its hygroscopic nature.
TiN 2 is a dark blue powder obtained when the oxide is ignited in an atmosphere of ammonia; while TiN is obtained as a bronze yellow mass as hard as the diamond by heating the oxide in an atmosphere of nitrogen in the electric furnace.
Thorpe), by heating to dull redness an intimate dry mixture of the oxide and ignited lamp-black in dry chlorine.
Coal dust alone, without any gas, may cause a dangerous explosion if ignited by a blown-out shot; but such cases are likely to be exceptional.
Having its ignition point below that of ordinary gas, it can be ignited by any redhot carbonaceous matter, such as the brightly glowing end of a cigar.
Whilst alcohol is applied in motor engines in a similar manner to petrol, its vapour mixed with a proper proportion of air being drawn into the cylinder where it is compressed and ignited, it cannot be used with maximum efficiency by itself in engines such as are fitted to modern motors because it requires a higher degree of compression than petrol engines are usually designed to stand, and also because, unless special arrangements are made, a motor engine will not start readily from the cold with alcohol alone.
To obtain the anhydrous single or double chloride, alumina must be ignited with carbon in a current of chlorine, and to exclude iron from the finished metal, either the alumina must be pure or the chloride be submitted to purification.
The filtrate, now containing roughly two molecules of alumina to one of soda, is concentrated to the original gravity of 1.45, and employed instead of fresh caustic for the attack of more bauxite; the precipitate is then collected, washed till free from soda, dried and ignited at about looo C. to convert it into a crystalline oxide which is less hygroscopic than the former amorphous variety.
This powder, provided that it has not been too' strongly ignited, is soluble in strong acids; by ignition it becomes denser and nearly as hard as corundum; it fuses in the oxyhydrogen flame or electric arc, and on cooling it assumes a crystalline form closely resembling the mineral species.
He attempted, not without success, to give a scientific account of eclipses, meteors, rainbows and the sun, which he described as a mass of blazing metal, larger than the Peloponnesus; the heavenly bodies were masses of stone torn from the earth and ignited by rapid rotation.
These, when reduced to their most simple expression, are mere basin-shaped hollows in the ground, containing ignited charcoal and the substances to be heated, the fire being urged by a blast of air blown in through one or more nozzles from a bellows at or near the top. They are essentially the same as the smith's forge.
The metal sinks through the ignited fuel, forming, in the hearth, a spongy mass or ball, which is lifted out by the smelters at the end of each operation, and carried to the forge hammer.
Instead of heating the tube, the gas may be ignited at the mouth of the tube and a cold surface of porcelain or platinum placed in the flame, when a black deposit is formed on the surface.
It is then allowed to stand twenty-four hours, filtered, washed with dilute ammonia, dried, ignited to constant weight and weighed, the filter paper being incinerated separately after moistening with nitric acid.
The mixture, then, was composed of such materials as sulphur and naphtha with quicklime, and took fire spontaneously when wetted - whence the name of wet fire or sea fire; and portions of it were "projected and at the same time ignited by applying the hose of a water engine to the breech" of the siphon, which was a wooden tube, cased with bronze.
The lead sulphate, re-precipitated in the filtrate by an excess of sulphuric acid and alcohol, is then filtered on an asbestos felt in a Gooch crucible, washed with dilute sulphuric acid and alcohol, ignited, and weighed.
Further, he showed that the spectrum of a dense ignited gas resembles that of an incandescent liquid or solid, and he traced a gradual change in the spectrum of an incandescent gas under increasing pressure, the sharp lines observable when it is extremely attenuated broadening out to nebulous bands as the pressure rises, till they merge in the continuous spectrum as the gas approaches a density comparable with that of the liquid state.
It is a pleasant-smelling gas, which burns when ignited, and may be condensed to a liquid which boils at 23.6° C. It is somewhat soluble in water and readily soluble in alcohol, and concentrated sulphuric acid.
To produce the alkali metal, a calcined mixture of sodium carbonate, coal and chalk was strongly ignited in flat retorts made of boiler-plate; the sodium distilled over into condensers and was preserved under heavy petroleum.
Potash-alum and pitch were calcined together, and the mass was treated with hydrochloric acid; charcoal and water to form a paste were next added, and the whole was dried and ignited in a current of air and steam.
Willstatter (Ber., 1904, 37, p. 4744), by dissolving pyrocatechin in absolute ether containing ignited sodium sulphate and then adding dry silver oxide, obtained the quinone in dark red crystalline plates which decompose between 60° and 70° C.
Prairie fires or spontaneous combustion have ignited many coal seams. Some have already burnt out; others still emit smoke and sulphurous fumes from the crevices in the hillsides, and through the fissures may be seen the glowing coal and rock.
Phosphorus is obtained as a soluble phosphate (which can be examined in the usual way) by lixiviating the product obtained when the substance is ignited with potassium nitrate and carbonate.