The residue on the filter paper gives (3) the substances insoluble in water.
A filter paper which has been previously heated to the temperature at which the substance is to be dried until its weight is constant.
If the precipitate settles readily, the supernatant liquor may be decanted through the filter paper, more water added to the precipitate and again decanted.
If, however, the precipitate refuses to settle, it is directly transferred to the filter paper, the last traces being removed by washing and rubbing the sides of the vessel with a piece of rubber, and the liquid is allowed to drain through.
It is washed by ejecting a jet of water, ammonia or other prescribed liquid on to the side of the filter paper until the paper is nearly full.
If the precipitate may be ignited, it is transferred to a clean, weighed and recently ignited crucible, and the filter paper is burned separately on the lid, the ash transferred to the crucible, and the whole ignited.
Knowing the weight of the crucible and of the ash of the filter paper, the weight of the precipitate is determined.
Into the solution dips a silver plate wrapped in filter paper, and the current is passed from the silver plate as anode to the bowl as cathode.
Once that is achieved, the sort of event that will happen is: You will be online to order, say, a replacement water filter, and the suggestion engine will propose that along with the filter, you might like to buy ... a pogo stick.
(a) Gravimetric. - This method is made up of four operations: (I) a weighed quantity of the substance is dissolved in a suitable solvent; (2) a particular reagent is added which precipitates the substance it is desired to estimate; (3) the precipitate is filtered, washed and dried; (4) the filter paper containing the precipitate is weighed either as a tared filter, or incinerated and ignited either in air or in any other gas, and then weighed.
If the substance to be weighed changes in composition on strong heating, it is necessary to employ a tared filter, i.e.
(4) After washing, the funnel containing the filter paper is transferred to a drying oven.
In the case of a tared filter it is weighed repeatedly until the weight suffers no change; then knowing the weight of the filter paper, the weight of the precipitate is obtained by subtraction.
The acid employed may be hydrochloric, which gives the best results, or sulphuric, which is used in Germany; sulphuric acid is more readily separated from the product than hydrochloric, since the addition of powdered chalk precipitates it as calcium sulphate, which may be removed by a filter press.
While he also prevents interruption of the operation by means of water-jackets, he uses hot-blast, and produces, besides metallic lead, large volumes of lead fumes which are drawn off by fans through long cooling tubes, and then forced through suspended bags which filter off the dust, called "blue powder."
Solutions of uranyl salts (nitrate, &c.) behave to reagents as follows: sulphuretted hydrogen produces green uranous salt with precipitation of sulphur; sulphide of ammonium in neutral solutions gives a black precipitate of UO 2 S, which settles slowly and, while being washed in the filter, breaks up partially into hydrated UO 2 an sulphur; ammonia gives a yellow precipitate of uranate of ammonia, characteristically soluble in hot carbonate of ammonia solution; prussiate of potash gives a brown precipitate which in appearance is not unlike the precipitate produced by the same reagent in cupric salts.
Generally it is either dried, after being separated from the wash water, by means of common salt, upon a layer of which the moist nitroglycerin is gently run and allowed to drain or filter through, or it is filtered through a mass of dry sponge or similar dry and porous material.
A modification of the system of double-bottom defecators has lately been introduced with considerable success in San Domingo and in Cuba, by which a continuous and steady discharge of clear defecated juice is obtained on the one hand, and on the other a comparatively hard dry cake of scum or cachaza, and without the use of filter presses.
These scums are not worth passing through the filter presses, and are sent to the fields direct as manure.
The juice is then drawn off and pumped up to one of the double-bottomed defecators and redefecated, or, where juice-heaters have been used instead of defecators, the scums from the separators or subsiders are heated and forced through filter presses, the juice expressed going to the evaporators and the scum cakes formed in the filter presses to the fields as manure.
In diffusion plants the milk of lime is added, in proper proportion, in the cells of the diffusion battery, and the chips or slices themselves act as a mechanical filter for the juice; while in the Sandwich Islands coral-sand filters have been employed for some years, in addition to the chips, to free the juice from impurities held in mechanical suspension.
The whole is then passed through filter presses, the clear juice being run off for further treatment, while the carbonate of lime is obtained in cakes which are taken to the fields as manure.
The filter presses remain substantially unchanged, although many ingenious but slight alterations have been made in their details.
The juice, which has now become comparatively clear, is again treated with lime, and again passed through a saturator and filter presses, and comes out still clearer than before.
The whole operation of thus changing a filter occupies about ten minutes, and there is no need for anyone to enter the hot cistern to detach the bags, which are removed in the open air above the mud tank.
The mud collects at the bottom of the u, and allows the upper part of the bag to filter for a longer time than would be the case if the bottom end were closed and if the bag hung straight like the letter I.
This weak solution, called " sweet water," is sometimes used for melting the raw sugar, or it is evaporated in a multiple-effect apparatus to 27° Beaume density, passed through the char filter, and cooked in the vacuum pan like the other liquors.
In the best-appointed refineries the whole of the work in connexion with the char is performed mechanically, with the exception of packing the filter cisterns with fresh char and emptying the spent and washed char on to the carrying bands.
It may also be precipitated as zinc ammonium phosphate, NH4ZnP04, which is weighed on a filter tared at 100°.
The modern distilling plant consists of two main parts termed the evaporator and condenser; in addition there must be a boiler (sometimes steam is run off the main boilers, but this practice has several disadvantages), pumps for circulating cold water in the condenser and for supplying salt water to the evaporator, and a filter through which the aerated water passes.
The filter is either a separate piece of plant, or, as in the Quiggins form, it may be placed below the coils in the same outer vessel.
The suggestion that it is due to the oxidation of a body excreted by the bacteria seems answered by the failure to filter off or extract any such body.
These toxins may become free in the culture fluid, and the living bacteria may then be got rid of by filtering the fluid through a filter of unglazed porcelain, whose pores are sufficiently small to retain them.
The separation of organic substances by filtration under high pressure through a colloid membrane, gelatine supported in the pores of a porcelain filter being usually employed.
When oxidation is complete the crude anthraquinone is separated in filter presses and heated with an excess of commercial oil of vitriol to 120° C., the various impurities present in the crude material being sulphonated and rendered soluble in water, whilst the anthraquinone is unaffected; it is then washed, to remove impurities, and dried.
AA, Tower; B, ammoniacal carbonate, which brine main; E, gas-inlet; Z, vacuum filter; always contains some V, pipe to air pump.
Hawley employs sodium thiostannate which precipitates thallium as T1 2 SnS 4, insoluble in water, and which may be dried on a Gooch filter at 105°.
By passing over or through rich soil the water may, however, actually be enriched, just as clear water passed through a charcoal filter which has been long used becomes impure.
After two or three hours the liquid is diluted till its density falls to 1.23, when it is passed through filter-presses to remove the insoluble ferric oxide and silica.
Continuous use of a periscope is very trying for the observer's eyes, and for use in bright weather light-filter screens are provided to reduce the glare.
In the form of a chromate, it may be determined by precipitation, in acetic acid solution, with lead acetate; the lead chromate precipitate collected on a tared filter paper, well washed, dried at loo° C. and weighed; or the chromate may be reduced by means of sulphur dioxide to the condition of a chromic salt, the excess of sulphur dioxide expelled by boiling, and the estimation carried out as above.
A fragment thrown on the surface of water rapidly disengages hydrogen, which gas, however, does not inflame, as happens with potassium; but inflammation occurs if hot water be used, or if the metal be dropped on moist filter paper.